Precision of the measurements was ± 0.5 ‰ for δD and ± 0.1 ‰ for δ 18O.įig. The samples were analysed for δD and δ 18O on the same aliquot by twin mass spectrometers designed for simultaneous analysis ( Reference Hagemann and LohezHagemann and Lohez, 1978). The ices were allowed to melt completely before being transferred, in the same way as the water samples, into glass bottles. ![]() The samples covered the freezing ranges from 0 to 10%, 10 to 20%, 20 to 50%, 50 to 60%, 60 to 70%, 70 to 80%, 80 to 90%, and above 90% for the last slice. When the freezing process was complete, the ice core was recovered and sectioned. Residual water was sampled at the beginning of the experiment, after 40%, 80%, 85%, 90% and 95% of the material had frozen. During each experiment, one millilitre of water was collected five times using a capillary tube inserted through the adjacent tube into the remaining water present in the cylinder. The freezing front moved downwards as a well-defined macroscopic plane. The residual water was continuously stirred during freezing with a small magnetic stirrer reasons for this stirring will be explained later. Excess water produced during freezing was diverted through an adjacent tube and allowed to escape. In each experiment, 500 ml of water was progressively frozen downwards in a “Plexiglass” cylinder of approximate dimensions 10 cm h and 8 cm internal diameter ( Fig. The changes during the course of freezing in δD and δ 18O of water samples and ice layers were determined by experiments on progressive unidirectional freezing. The aim of this paper is to test this model experimentally. This freezing effect has been developed theoretically for a closed system and applied to practical case. We have shown ( Reference Jouzel and SouchezJouzel and Souchez, 1982) from practical studies of regelation ice and from theoretical studies, that, after melting and refreezing, ice samples lie on a straight lie on a straight line in a δD–δ 18O diagram, with a slope different from that of the precipitation effect. ![]() This trend, also valid for glacier ice, is recognized in the literature as being an important feature of the isotopic fractionation of water occurring during condensation or sublimation in simple equilibrium processes ( Reference Craig, Craig, Gordon and HoribeCraig and others, 1963 Reference DansgaardDansgaard, 1964) it is called the precipitation effect. In this equation, as in those presented in this paper, δD and δ 18O are expressed in parts per thousand of the standard mean ocean water (S.M.O.W.) with D/H and 18O/ 16O equal to 155.76 × 10 −.2 × 10 −6 respectively. Detailed studies of the relationships between isotopic species in ice and water have established that δD = 8δ 18O + 10 in fresh precipitation of all types and in most surface waters.
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